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Single crystals of NaBa 3 RuO 6  (I) and NaBa 3 IrO 6  (II) have been prepared by crystallization from melts in closed silver tubes. The crystal structures were investigated by X-ray techniques. Both compounds crystallize with trigonal (rhombohedral) symmetry, space group D 6  3d -R3̅c, I: a = 10.107(2), c = 11.872(2) Å, II: a = 10.128(2), c = 11.905(2) Å, Z = 6. I and II are isostructural to the Sr 4 PtO 6  type.

zeitschrift für naturforschung b

Notizen:Über NaBa 3 RuO 6 und NaBa 3 IrO 6 .Zwei Edelmetall-Oxometallate mit Sr 4 PtO 6 -Struktur / On NaBa 3 RuO 6 and NaBa 3 IrO 6 .Two Noble Metal Oxometallates Showing Sr 4 PtO 6 Structure