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The reaction of trifluoroacetylacetone with salicylhydrazone gives acetone salicylhydra­ zone besides the expected trifluoroacetylacetone salicylhydrazone. The resulting mixture was analyzed by mass spectroscopy. The structure of acetone salicylhydrazone was determined by X-ray analysis. Crystal data: a = 12,8493(12) Å, b = 6,1084(8) Å, c = 12,757(3) Å; space group Pna2 1 ; Z = 4; R = 0,051 ; 750 unique reflexions.

Hydrolyse von Trifluoracetylaceton-salicylhydrazon / Hydrolysis of Trifluoroacetylacetone Salicylhydrazone: Struktur von Aceton-salicylhydrazon /