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Single crystals of K 4 CdV 5 O 15 Cl have been prepared by crystallization from melts. The yellow crystals show tetragonal symmetry, space group C 1  4 -P4, a = 9.097(1), c = 5.331(2) Å, Z = 1. K 4 CdV 5 O 15 Cl belongs to the K 4 CuV 5 O 3 Cl type. V (l) forms V 2 O 7  double tetrahedra connected by square V(2)O 5  pyramids and CdO 4 Cl 2  octahedra. The crystal structure is dis­cussed with respect to the isotypic compound K 4 CuV 5 O 15 Cl considering a short V(2)-O distance indicative of a vanadinyl group.

zeitschrift für naturforschung b

Zur Kenntnis des ersten Alkalimetall-Cadmium-Halogeno-Oxovanadats: K 4 CdV 5 O 15 Cl / On the First Alkaline-Cadmium-Vanadium Oxide Halide: K 4 CdV 5 O 15 Cl