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Single crystals of (I) CuDyMo 2 O 8  and (II) CuYbMo 2 O 8  have been prepared by crystalli­sation from melts. Both com pounds crystallize with orthorhombic symmetry, space group D 15  2h -Pbca with (I): a = 10.195(1), b = 9.721(2), c = 14.563(3); (II): a = 10.094(6), b = 9.628(9), c = 14.467(8) Å, Z = 8. The crystal structure is characterized by a triangular CuO 3 -polygon, a square antiprismatic coordination around the Rare Earth ions and the typical Mo O 4  tetra­ hedra.

Zur Kristallchemie von CuDyMo 2 O 8 und CuYbMo 2 O 8