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(MePh 3 P) 2 l 8  has been prepared by the reaction of methyltriphenylphosphonium iodide with iodine in ethanol. It crystallizes in the monoclinic space group P2 1 /n with a = 985.2(2), b = 1260.0(1), c = 1872.6(4) pm, β = 91.50(2)° and Z = 4. The crystal structure has been refined to R = 0.030 for 2882 reflections. It may be described as a layerlike packing of cations and anions. The anion with point symmetry 1̅ consists of two triiodide groups and a bridging iodine molecule forming a rather common nearly planar Z-shaped octaiodide ion I 8  2- .

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Untersuchungen an Polyhalogeniden, XIX [1] Bis(methyltriphenylphosphonium)oktaiodid (MePh 3 P) 2 I 8 , Cäsium(18-Krone-6)triiodid [Cs(C 12 H 24 O 6 )]I 3 , Iodoblei(18-Krone-6)triiodid [Pb(C 12 H 24 O 6 I]I 3  und Diiodothallium(18-Krone-6)tetraiodothallat [Tl(C 12 H 24 O 6 )I 2 ](TlI 4 ) / Studies of Polyhalides, XIX [1] Bis(methyltriphenylphosphonium) Octaiodide (MePh 3 P) 2 I 8 , Cesium(18-crown-6) Triiodide [Cs(C 12 H 24 O 6 )]I 3 , Iodolead(18-crown-6) Triiodide [Pb(C 12 H 24 O 6 )I]I 3  and Diiodothallium(18-crown-6) Tetraiodothallate [Tl(C 12 H 24 O 6 )I 2 ](TlI 4 )