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The reaction of Cp 2 ZrCl{P(SiMe 3 ) 2 } with aniline yields the terminal zirconocene phenylamido complex Cp 2 ZrCl(NHPh) (1) and HP(SiMe 3 ) 2 . 1 was characterized spectroscopically (n.m.r., i.r.) and by X-ray structure determination (monoclinic space group P 2  {ln, a - 6.589(2), b = 19.978(3), c = 13.512(2) Å , β = 101.09(2)° (at 200 K)). The NHPh group is planar with Zr -N 2116(10) Å.

zeitschrift für naturforschung b

Aminolyse von Cp 2 ZrCl{P(SiMe 3 ) 2 } - Synthese und Molekülstruktur von Cp 2 ZrCl(NHPh) / Aminolysis of Cp 2 ZrCl{P(SiMe 3 ) 2 } - Synthesis and Molecular Structure of Cp 2 ZrCl(NHPh)