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[{Ru(CO) 3 Cl 2 } 2 ] reacts with the in situ prepared reagent Li 2 [Fe(CO) 3 (PBu t  2 ) 2 ] to give the new heterobinuclear complex [FeRu(CO) 5 (μ-PBu t  2)2 ] (1). Crystals of 1 are isomorphous to those of the known compound [Fe 2 (CO) 5 (μ-PBu t  2 ) 2 ] (2) and crystallize in the triclinic space group P1̄ with a = 867,5(1), b = 1181,0(2), c = 1373,1(2) pm; α = 76,64(1), β = 79,72(1) and γ = 76,48(1)°. A double bond between the two metal atoms concluded for 2 from the results of EHMO calculations is also proposed for 1 (Fe=Ru: 259,8(1) pm).

zeitschrift für naturforschung b

Synthese und Kristallstruktur des koordinativ ungesättigten Komplexes [FeRu(CO) 5 (μ-PBu t  2 ) 2 ] / Synthesis and Crystal Structure of the Coordinatively Unsaturated Complex [FeRu(CO) 5 (μ-PBu t  2 ) 2 ]