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Preparation and crystal structure of [P(C 6 H 5 ) 4 ]Cl 3  are reported. [P(C 6 H 5 ) 4 ]Cl 3  crystallizes in the monoclinic space group P2 1/ c with a = 1093.4(4), b = 789.1(1), c = 2682.7(7) pm, β = 90.39(1)°, V = 2200.27·10 6  pm 3 , and Z = 4. The geometry of the trichloride anion in the solid state is almost linear (Cl-Cl-Cl = 178.44(4)°) and unsymmetrical (d(Cl-Cl) = 226.3(1) and 230.7(1) pm).

Darstellung und Kristallstruktur von [P(C 6 H 5 ) 4 ]Cl 3 / Preparation and Crystal Structure of [P(C 6 H 5 ) 4 ]Cl 3