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Single crystals of Rb 0.6 K 0.4 CuMo 3 O 10  have been prepared by crystallization from melts and investigated by X-ray diffractometer technique. They crystallize with orthorhombic symmetry, space group D 2h  16  -Pnma , a = 8.606(2), b = 7.595(3), c - 13.660(7) Å, Z = 4. The crystal structure of Rb 0.6 K 0.4 CuMo 3 O 10  is characterized by the rare octahedral coordination of molybdenum and is related to (NH 4 ) 2 Mo 3 O 10  with respect to the one-dimensional  1  ∞ [Mo 3 O 10 ]- chains.

zeitschrift für naturforschung b

Ein Beitrag zur Synthese und Kristallchemie des Alkalimetall-Kupfer -Oxomolybdats Rb 0,6 K 0,4 CuMo 3 O 10  / A Contribution on the Synthesis and Crystal Chemistry of the Alkaline Copper Oxomolybdate Rb 0.6 K 0.4 CuMo 3 O 10