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Me 3 CSiHal 3  react with LiOCMe 3  to give Me 3 CO(Me 3 C)SiHal 2  (HaI = F (1), Cl (3)). The aminofluorosilane, Me 3 CO(Me 3 C)SiFNH 2  (2), is formed in the reaction of 1 with LiNH 2 . The diaminosilane Me 3 CO(Me 3 C)Si(NH 2 ) 2  (4) is obtained from the reaction of 2 with ammonia. 4 reacts with LiC 4 H 9  to give the lithium derivative Me 3 CO(Me 3 C)Si(NHLi)NH 2  (5). In a molar ratio 1:1 the reaction of 5 and 1 leads to the formation of the 1-amino-3-fluoro-disilazane Me 3 CO(Me 3 C)SiF- NH - SiNH 2 (CMe 3 )OCMe 3  (6) and in a molar ratio 2:1 to the four-membered silicon nitrogen ring [Me 3 CO(M e 3 C)Si-NH] 2  (7). The crystal structure of 7 was determined.

zeitschrift für naturforschung b

Synthese und Kristallstruktur des 2.4-Di-terf-butoxy-2,4-di-terfbutylcyclodisilazans / Synthesis and Crystal Structure of 2.4-Di-terf-butoxy-2,4-di-terrbutylcyclodisilazane