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Preparation and spectroscopic data of the new compounds Si 3 O 3 (NHCH 3 ) 6  (1), Si 3 O 2 (NCH 3 )(NHCH 3 ) 6  (2 ), (CH 3 ) 3 Si-NCH 3 -Si 2 OCl 5  (3 ), ((CH 3 ) 3 Si-NCH 3 ) 2 Si 2 OCl 4  (4) and [Cl 3 Si-O-SiCl 2 -NCH 3 -AlCl 2 ] 2  (5) are reported. The structure of the chlorinated alummosiloxazane compound has been determined by single crystal X-ray analysis (space group P1̄, a = 8,357(1), b = 9,538(1), c = 9,774(1) Å, α = 85,35(1), β = 65,39(1), γ = 71,97(1)°, 2620 data (F 0  &gt; 3σ(F 0 ), R = 0,040). The molecule shows a dimetric structure and contains a planar four-membered Al 2 N 2  ring with Si 2 OCl 5  groups in trans-position.

Kondensationsfähige Si–N–Verbindungen zum Aufbau poröser Festkörper