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By electrochemical oxidation of [B 6 H 6 ] 2-  in the presence of nitrite ions and of the base DBU in dichlorom ethane solution the μ-nitroso-bis(pentahydrohexaborate) [B 6 H 5 (NO)B 6 H 5 ] 3-  ion is formed and can be isolated by ion exchange chromatography on diethylaminoethyl cellulose. The crystal structure of the Cs salt has been determined from single crystal X-ray diffraction analysis. Cs 3 [B 6 H 5 (NO)B 6 H 5 ] is orthorhombic, space group Pnma with a = 16.2303(13), b = 12.245(6), c = 25.444(2) Å. The unit cell contains three crystallographically independent anions with nearly C 2v  symmetry but differently distorted B 6  cages

zeitschrift für naturforschung b

Darstellung von μ-Nitroso-bis(pentahydro-closo-hexaborat)(3-) und Kristallstruktur von Cs 3 [B 6 H 5 (NO)B 6 H 5 ] / Preparation of μ-nitroso-bis(pentahydro-closo-hexaborate)(3-) and crystal structure of Cs 3 [B 6 H 5 (NO)B 6 H 5 ]