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Crystals of KCoPO 4  were obtained by growth in a gel of tetramethoxysilane/water at 64 °C. The hexagonal crystals have space group P6 3 , a = 18.206(1), c = 8.5135(8) [Å], V = 2443.8(4) [Å 3 ]. Z = 24. The structure was solved by single crystal X-ray diffraction methods. The structure is isotypic with α-KZnPO 4 . It comprises an ordered three dimensional network of alternating CoO 4  and PO 4  tetrahedra. which has rings of six tetrahedra in the xy plane. These rings form tunnels in the [001] direction, where the potassium ions are located. Upon heating, the compound undergoes a phase transition at about 565 °C; on cooling, the phase transition occurs at 449 °C, where it transforms into another structure which is yet unknown. This indicates that the hexagonal structure is a metastable phase

Crystal Growth and X-Ray Structure of Metastable α-KC0 PO 4