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Cu 6 Br 6 (NPMe 3 ) 4  has been prepared as a by-product from the reaction of CuBr with Me 3 SiNPMe 3  in a CH 2 Cl 2  suspension. The dark red-violet crystals, which contain three molecules CH 2 Cl 2  per unit cell, have been characterized by a crystal structure determination.

Cu 6 Br 6 (NPMe 3 ) 4 , ein gemischt-valenter Kupfercluster / Cu 6 Br 6 (NPMe 3 ) 4 , a Mixed-Valent Cluster of Copper