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The preparation of the thiosulfonium salts (CH 3 ) 2 SSSH + SbF 6  -  and (CH 3 ) 2 SSSCH 3  + SbCl 6  -  from (CH 3 ) 2 SSCl + SbF 6  -  and (CH 3 ) 2 SSH + SbCl 6  - , resp., at 195 K is reported. (CH 3 ) 2 SSSH + SbF 6  -  is transformed into (CH 3 ) 2 SSSCl + SbF 6  -  by reaction with Cl 2  at low temperatures. The salts have been characterized by their Raman spectra

zeitschrift für naturforschung b

Uber die Darstellung von (CH 3 ) 2 SSSH + SbF 6  - und (CH 3 ) 2 SSSCH 3  + SbCl 6  - [1] / On the preparation of (CH 3 ) 2 SSSH + SbF 6  -  and (CH 3 ) 2 SSSCH 3  + SbCl 6  - [1]