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The reaction of trimethylamine, H 2 S, and sulfur in ethanol yields orange crystals of bis(trimethylammonium) hexasulfide. The com pound crystallizes in the centrosymmetric monoclinic space group P 2/c. The lattice constants are a = 10.310(7), b = 5.752(2), c = 13.348(10) Å, β = 98.41(6)°. The S 2  6 -chain has a helical all-trans-conformation (sequence of the signs of torsion angles +++ and --- ).

zeitschrift für naturforschung b

Darstellung und Kristallstruktur des Bis(trimethylammonium)hexasulflds [HN(CH 3 ) 3 ] 2 S 6  / Preparation and Crystal Structure of Bis(trimethylammonium)hexasulfide [HN(CH 3 ) 3 ] 2 S 6