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The reaction of [VO(dipic)(H 2 O) 2 ]·2H 2 O with benzoylhydrazine, thiobenzoylhydrazine and O-methylcarbazate yields [V(dipic)(NH 2 NHCOPh)(H 2 O)2][VO(dipic)(NHNCOPh)·2H 2 O (1), [V0(dipic)(NHNHCO 2 Me)] (2), [VO(dipic)(NH 2 NHCO 2 Me)] (3) and [VO(dipic)(NHNHCSPh)] (4). 1 is probably formed in solution by redox disproportionation. The reactions giving 2,3 and 4 also involve redox processes with atmospheric oxygen as oxidant and the respective hydrazine as reductant. [VO('ONO')(NHNHCOPh)]·H 2 O (5) was formed using aqua-oxo-salicylaldehyde-L-alaninato-vanadium(IV) as precursor. The structures of 1,2,3 and 5 have been determined by single crystal X-ray crystallography.

zeitschrift für naturforschung b

Derivate des Hydrazins als Liganden in Vanadium(III)-, -(IV)- und -(V)-Komplexen. Darstellung und Charakterisierung von [V(dipic)(NH 2 NHCOPh)(H 2 O) 2 ][VO(dipic)(NHNCOPh)]·2H 2 O , [VO(dipic) (NHNHCO 2 Me)], [VO(dipic)(NH 2 NHCO 2 Me)], [VO(dipic)(NHNHCSPh)] und [VO('ONO')(NHNHCOPh)]·2H 2 O / Substituted Hydrazines as Ligands in Vanadium(III), -(IV) and -(V) Complexes. Synthesis and Characterization of [V(dipic)(NH 2 NHCOPh)(H 2 O) 2 ][VO(dipic)(NHNCOPh)]·2H 2 O , [VO(dipic) (NHNHCO 2 Me)], [VO(dipic)(NH 2 NHCO 2 Me)], [VO(dipic)(NHNHCSPh)] und [VO('ONO')(NHNHCOPh)]·2H 2 O