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We report the synthesis of 3,5-di-tert-butylstyrene (5). The alkylation of toluene with tertbutylchloride establishes the 1,3,5-substitution pattern. A Wittig reaction introduces the C 1  unit. This and similar bulky styrene derivatives will be used as special building blocks for polymer design.

3.5-Di-tert-butylstyrole: Synthese sterisch anspruchsvoller Polymerbausteine / 3.5-Di-tert-butylstyrenes: Synthesis of Bulky Polymer Building Blocks