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Gd 2 (SO 3 ) 3  • 3 H 2 0 is obtained by passing gaseous SO 2  through a suspension of Gd 2 O 3  in H 2 O at room temperature until a clear solution is formed. Single crystals are obtained by heating to 70(2) °C for 6 days. The compound crystallizes in the triclinic space group P 1 with a = 6.499(6), b = 6.621(3), c = 6.954(3) Å, α = 110.71(5), β = 90.54(3), γ = 106.05(1)° and Z = 1.

zeitschrift für naturforschung b

Die Kristallstruktur von Gadolinium (III)-sulfit Trihydrat Gd 2 (S0 3 ) 3 ∙ 3H 2 O / Crystal Structure of Gadolinium(III)-sulfite Trihydrate Gd 2 (SO 3 ) 3  ∙3H 2 O