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The title compounds were prepared from chloro(organophosphine)metal(I) complexes and the urea homologues SeC(NH 2 ) 2  and SC(NHMe) 2  in good yields. Recrystallization of [Ph 3 ,PAg{SeC(NH 2 ) 2 }] + Cl -  from DMF/CH 2 Cl 2  leads in low yield to the dinuclear complex [{µ 2 -SeC(NH 2 ) 2 }Ag{SeC(NH 2 ) 2 } 2 ] 2  2+ 2Cl -  • 4DMF. The crystal structure reveals short Ag-Ag contacts and unexpectedly acute angles at the bridging selenium atom. The crystal structure of [Ph 3 PAu{SC(NHMe) 2 }] + Cl -  • SC(NHMe) 2  shows short N•••Cl and N•••S contacts that probably correspond to hydrogen bonding.

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Complexes of Copper, Silver, and Gold with Urea Homologues. Crystal Structures of [{µ 2 -SeC(NH 2 ) 2 } Ag{SeC(NH 2 ) 2 } 2 ] 2  2+ 2Cl -  • 4 DMF and [Ph 3 PAu{SC(NHMe) 2 }] + Cl -  • SC(NHMe) 2