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The new compound Y 7 I 6 C 3 O is prepared by reaction of stoichiometric amounts of Y, YI 3 , Y 2 O 3  and C in closed Ta capsules at 1370 K. Y 7 I 6 C 3 O forms bronze coloured, metallic, air and moisture sensitive crystals. It crystallizes in the space group Pmma (No. 51) with the lattice constants a = 2249.4(4), b = 383.7(1), c = 1079.1(1) pm. Within the crystal structure the C atoms and the O atoms are surrounded by Y atoms octahedrally and tetrahedrally, respectively. The Y 6 C octahedra and Y 4 O tetrahedra are condensed to form ondulated layers, which are separated by double layers of I atoms.

zeitschrift für naturforschung b

Notizen: Y 7 I 6 C 3 O: Ein Carbidoxid mit kondensierten Y 6 C-Oktaedern und Y 4 O-Tetraedern / Y 7 I 6 C 3 O: A Carbide Oxide with Condensed Y 6 C-Octahedra and Y 4 O-Tetrahedra