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fac-Li 4 [Rh(SO 3 ) 3 (OH 2 ) 3 ](OH) crystallizes in the rhombohedral space group R3-C 3  4 , Z = 1, in trigonal setting a = 807.7(2), c = 1339.0(3) pm, V = 756.6(2)· 10 6  pm 3 , Z = 3. Rh is octahedrally coordinated by three facial S-bonded sulfite groups with Rh—S = 222.6(1) pm and three aqua ligands with Rh—O bonds Rh—O = 217.5(3) pm, elongated by a trans-influence. The average S—O bond length is 148.0(3) pm. All hydrogen atoms have been located. The OH -  ion is coordinated exclusively to Li+. The anions are held together by Li +  cations in octahedral environment and by hydrogen bonds of medium strength. Alternatively, the structure can be considered to be built of packages of two oxygen nets and a metal layer, stacked in a sequence similar to that in the CdCl 2 -structure.

The Crystal Structure of Lithium fac-Triaquatrisulfitorhodate(III)hydroxide, Li 4 [Rh(S0 3 ) 3 (OH 2 ) 3 ](OH)