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Crystals of the complexes [CdI 2  · C 6 H 12 S 3 ] 2  (1) and [Hg(C 6 H 12 S 3 ) 2 ](HgI 3 ) 2  (2) were obtained by diffusion of 1,4,7-trithiacyclononane (9 S 3) in ethanol into aqueous solutions of cadmium iodide and mercuric iodide/potassium iodide, resp. Both compounds crystallize monoclinically,1: space group P2 1 /n, Z = 4, a = 1207.1(5), b = 909.9(2), c = 1240.3(7) pm, β = 92.59(9)°; 2: P2 1 /c, Z = 2, a = 804.7(6), b = 934.0(6), c = 2167.9(4) pm, β = 94.34(7)°. 1 is dimeric, consisting of two [CdI 2  · 9S3] units, connected via iodine bridges. Crystals of 2 contain sandwich-like cations [Hg(9S3) 2 ] 2+  and [HgI 3 ] -  anions, forming chains via Hg ··· S and Hg ··· I bridges.

zeitschrift für naturforschung b

Metallkomplexe mit 1,4,7-Trithiacyclononan: Kristallstrukturen von [CdI 2  · C 6 H 12 S 3 ] 2  und [Hg(C 6 H 12 S 3 ) 2 ](HgI 3 ) 2  / Metal Complexes with 1,4,7-Trithiacyclononane: Crystal Structures of [CdI 2  · C 6 H 12 S 3 ] 2  and [Hg(C 6 H 12 S 3 )2](HgI 3 ) 2