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The diamagnetic tetranuclear cluster complexes Mo 3 CuS 4 I(R 2 PS 2 ) 4 •C 5 H 5 N 2 (a: R=Et, b: R=Pr) are obtained by reaction of Mo 3 S 4 L 4  (L = R 2 PS 2- ) 1 with CuI and pyridine. Each Mo atom of the cubane-type Mo 3 CuS 4  core is chelated by L. Two of the Mo atoms are bridged by the fourth L, while a pyridine ligand completes the coordination sphere of the third Mo atom, and iodine is bonded to the Cu atom. Magnetic, NMR- and MS-spectroscopic data are given. 2b crystallizes in the monoclinic space group P2 1 /n with Z = 4 and lattice parameters a = 21,164(7), b = 10,653(3), c = 25,455(8)Å, and β = 106,25(3)°.

zeitschrift für naturforschung b

Synthese, Struktur und Eigenschaften von kubanartigen Molybdän-Kupfer-Schwefel-Cluster-Dithiophosphinaten / Synthesis, Structure, and Properties of Cubane-Type Molybdenum-Copper-Sulfur Cluster Dithiophosphinates