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Aquacopper(II) glycyl-β-alaninate (1) and aquacopper(II)-β-alanylglycinate (2) were obtained from CuCO 3  and the appropriate dipeptide under reflux in water. 2 crystallizes in the orthorhombic space group Pna2 I . The lattice constants (291 K) are: a = 8.984(2), b = 12.456(2), c = 6.978(2) Å. The dipeptide anion, acting as a tridentate ONN ligand, and one oxygen atom of the carboxylate group of a neighbouring molecule form the base of a square pyramid around Cu, with water in the apical position. Cu is found slightly above the base. The molecules are connected by bridging carboxylate groups to form chains which are linked by hydrogen bonds between the water molecule and the oxygen atom of the peptide group.

zeitschrift für naturforschung b

Darstellung und Charakterisierung von Kupfer(II)-Derivaten des Glycyll-β-alanins und des β-Alanylglycins. Kristallstruktur von Cu(II)-ßAlaGly • H 2 O / Preparation and Characterization of Copper(II) Derivatives of Glycyl-β-alanine and β-Alanylglycine. Crystal Structure of Cu(II)-β-AlaGly • H 2 O