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Different hydrates of Gd 2 (SO 3 ) 3  are obtained depending on preparation conditions. For preparation of Gd 2 (SO 3 ) 3 , gaseous SO 2  is passed through a suspension of Gd 2 O 3  in H 2 O at room temperature until a clear solution is formed. Upon immediate heating to about 100 °C a mixture of Gd 2 (SO 3 ) 3  · 2H 2 O and Gd 2 (SO 3 ) 3  · 3H 2 O is formed. If the boiling procedure is performed after 6 days, a pure product consisting of the trihydrate is obtained. The different phases are identified by REM, DTA -TG -investigation and X-ray powder analysis. The X-ray powder pattern of Gd 2 (SO 3 ) 3  · 2H 2 O is consistent with patterns of isotype Ln 2 (SO 3 ) 3  · H 2 O were Ln = Pr, Nd, Sm and Eu.

zeitschrift für naturforschung b

Zur Kenntnis von Gadolinium(III)-sulfit Dihydrat Gd 2 (SO 3 ) 3 · 2 H 2 O/ On the Existance of Gadolinium (III)-sulfite Dihydrate Gd 2 (SO 3 ) 3  · 2H 2 O