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The structures of two polymeric complexes of chromium(III) azide with pyridine, KCr(py) 4 (N 3 ) 4  (1), and RbCr(py) 3 (N 3 ) 4  (2), were determined by X-ray crystallography. Crystal data: 1, C 20 H 20 N 16 CrK, monoclinic, space group C2/c, a = 1611.2(5), b = 1050.6(3), c = 1609.0(5) pm, β = 91.69(3)°, Ζ = 4 and Rw = 0.037 for 923 diffractometer data; 2, C 15 H 15 N 15 CrRb, monoclinic, space group P2 1 /n, a = 1311.9(3), b = 1139.0(4), c = 1523.3(4) pm, β = 109.39(2)°, Ζ = 4 and R w  = 0.046 for 2336 data.

zeitschrift für naturforschung b

Crystal Structure Investigation of Two Polymeric Chromium(III) Azide Complexes; KCr(pyridine) 4 (N 3 ) 4  and RbCr(pyridine) 3 (N 3 ) 4 . A Structure Containing μ(l,3) and μ(1,1,3) Bridging Azido Ligands between Chromium and Rubidium Centered Polyhedra