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The thallium(I)-2-pyridyl-cyanoxime complex was prepared in a 82% yield. An X-ray crystallographic study of C 7 H 4 N 3 OT1 (Space group P2 1 /c, a = 4.134(1), b = 8.875(2), c = 22.217(6) Å, β = 92.55(2)°, Ζ = 4, R = 4.36%, wR = 3.94% for 930 reflections) showed that the complex contains thallium(I) in a trigonal bipyramidal arrangement.

Preparation, IR and X-Ray Crystal Structure Studies of Tl(I)-2-pyridyl-cyanoxime Complex