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Pale yellow crystals of LiBa 4 [Mo 2 N 7 ] • BaCl 2  (monoclinic, P2 1 /m; a = 1113.5(3), b = 605.8(1), c = 1122.7(3) pm; β = 95.65(2)°; Z = 2) were grown from the melt (LiCl/Ba 3 [MoN 4 ], molar ratio 3:1, T max  = 1050 °C) by cooling (5°C/h). The crystal structure contains dimeric units [Mo 2 N 7 ] 9-  (eclipsed conformation; N-Mo-N: 173.7°; Mo-N (term.) : 182.7(5)-186.1(8) pm; Mo-N (bridg.) : 190.6(8) and 192.3(8) pm).

zeitschrift für naturforschung b

LiBa 4 [Mo 2 N 7 ] • BaCl 2 : Dimere Anionen [Mo 2 N 7 ] 9-  durch Kondensationsreaktion von Ba 3 [MoN 4 ] in LiCl-Schmelzen / LiBa 4 [Mo 2 N 7 ] • BaCl 2 : Dimeric Anions [Mo 2 N 7 ] 9-  by Condensation Reaction of Ba 3 [MoN 4 ] in LiCl Melts