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Zn(pymt) 2  and Cd(pymt) 2  complexes have been obtained by electrochemical oxidation of anodic zinc or cadmium in acetonitrile solutions of pyrimidine-2-thione (Hpymt). When 2,2′-bipyridine (bipy) or 1,10-phenanthroline (phen) was added to the electrochemical cell, the adducts [M(pymt) 2 (bipy)], or [M(pymt) 2 (phen)] (M = Zn or Cd) were obtained. Crystals of [Cd(pymt) 2 phen] are orthorhombic, with a = 9.882(2), b = 12.491(1), c = 16.513(2)Å, space group P2 1 2 1 2 1  and Z = 4. The cadmium atom has distorted octahedral geometry, and one nitrogen atom of each pyrimidine-2-thiolato ligand is not coordinated.

zeitschrift für naturforschung b

Direct Electrochemical Synthesis of Pyrimidine-2-thionato Complexes of Zinc(II) and Cadmium(II): The Crystal Structure of (1,10-Phenanthroline)bis(pyrimidine-2-thionato)cadmium(II)