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Thermal decomposition of N 2 H 6 [CrF 5 (H 2 O)] has been investigated by thermoanalytical, X-ray and IR spectroscopic methods. Under quasi-isobaric conditions the decomposition takes place in several steps. The intermediate N 2 H 6 CrF 5  has been found which crystallizes monoclinically with α = 555.0 pm, b = 1084.6 pm, c = 777.0 pm, β = 91.76°. N 2 H 6 CrF 5  decomposes via an amorphous intermediate to give pure rhomboedrical CrF 3  as the final product. One of the intermediate has been identified as chromium fluoride ammoniate CrF 3  0.4 NH 3 . No hydrolysis reactions have been observed.

zeitschrift für naturforschung b

Über die thermische Zersetzung von N 2 H 6 [CrF 5 (H 2 O)] und die neue Verbindung N 2 H 6 CrF 5  / On the Thermal Decomposition of N 2 H 6 [CrF 5 (H 2 O)] and the New Compound N 2 H 6 CrF 5