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Transparent single crystals of Na 4 Ga 2 S 5  were obtained from a melt of Na 2 S, Ga and S. Na 4 Ga 2 S 5  is monoclinic, space group P2 1 /c with a = 7.967(1), b = 6.133(2), c = 19.852(9) Å, β = 91.61(2)°, Ζ = 4. Its crystal structure was refined to a conventional R of 0.033 for 1150 observed reflections.

zeitschrift für naturforschung b

Darstellung und Kristallstruktur von Na 4 Ga 2 S 5 . Ein Thiogallat mit       -Zweier-Doppelketten / Preparation and Crystal Structure of Na 4 Ga 2 S 5 . A Thiogallate with       --zweier-Double Chains