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NaNEt 4 S 4  was obtained from an equimolar solution of Na 2 S 4  and NEt 4 Cl in ethanol. Its crystal structure was determined by X-ray diffraction with 4175 observed unique reflexions, R = 0.044. Crystal data: a = 713.4(4), b = 1744.5(9), c = 1204.0(5) pm, β = 105.8(3)°, space group P2 1 /n, Ζ = 4. In the structure, chains consisting of Na +  and S 4  2−  ions run in the a direction, every Na +  being coordinated by four terminal S atoms of S 4  2−  ions (two terminal, one chelating). The chains are separated by the NEt 4  +  ions.

zeitschrift für naturforschung b

Natrium-tetraethylammonium-tetrasulfid, Na + NEt 4  + S 4  2− . Synthese und Kristallstruktur / Sodium Tetraethylammonium Tetrasulfide, Na + NEt 4  + S 4  2− . Synthesis and Crystal Structure