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Silvery reflecting melting cakes of PdS 1-x Se x  (0.0 ≤ x ≤ 1.0) have been prepared by annealing mixtures of Pd, S and Se at 873 K in evacuated quartz tubes. The PdS-type mixed crystals are stable only in the ranges 0.0 ≤ .x ≤ 0.2 and 0.9 ≤ x ≤ 1.0, whereas a new phase appears in the intermediate region. The new phase PdS 1-x Se x  (0.2 &lt; x &lt; 0.9) crystallizes in the space group P4 2 /mbc and Z = 24. Lattice constants are a = 1126.2(7), c = 683.2(7) pm (PdS 0.6 Se 0. 4) and a = 1130.8(9), c = 685.4(8) pm (PdS 0.4 Se 0.6 ). The relationships between the new structure type and the PtS and PdS structure types are discussed.

zeitschrift für naturforschung b

Röntgenographische, elektrische und spektroskopische Untersuchungen an den Palladiumchalkogeniden PdS 1-x Se x  / Roentgenographic, Electrical and Spectroscopic Investigations of the Palladium Chalcogenides PdS 1-x Se x