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The reaction of Cp*SiCl 3  with LiAl(PH 2 ) 4  yields the compound Cp*Si(PH 2 ) 3  (1) which rearranges in the reaction mixture at room temperature to give the new 1,3-diphospha-2,4-disilacyclobutane (1,3-diphospha-2,4-diseletane) [Cp*Si(PH 2 )PH] 2  (2). Compound 2 could be isolated in pure form and has been fully characterized by spectroscopic methods.

zeitschrift für naturforschung b

Beiträge zur Chemie des Phosphors, 220. [Cp*Si(PH 2 )PH] 2  - ein P- und Si-funktionelles 1,3-Diphospha-2,4-disilacyclobutan / Contributions to the Chemistry of Phosphorus, 220. [Cp*Si(PH 2 )PH] 2  - a P- and Si-Functionalized 1,3-Diphospha-2,4-disilacyclobutane