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The reaction of ClSO 2 N = PPh 2 Cl () with NH 3  yields H 2 NSO 2 N = PPh 2 NH 2  ( 2 ).This compound is converted to Me 3 Si(H)NSO 2 N = PPh 2 N(H)SiMe 3  ( 3 ) by Me 3 SiNMe 2 .  3  reacts with WOCl 4  under elimination of (Me 3 Si) 2 O and ClSO 2 NH 2  to yield the eight-membered ring system (Cl 3 WNPPh 2 N) 2  ( 4 ).The molecular structure of  4  was investigated by an X-ray structure analysis.

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Reaktion von N-Trimethylsilyl-N′(N″ -trimethylsilylammodiphenylphosphoranylidenimino) sulfamid mit Wolframoxitetrachlorid und die Struktur von (Cl 3 WNPPh 2 N) 2  Reaction of N-Trimethylsilyl-N′(N″ -trimethylsilylaminodiphenylphosphoranylidene)sulfamide with Tungstenoxitetrachloride and the Structure of (Cl 3 WNPPh 2 N) 2