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In order to elucidate specific properties of nickel sulfur complexes, reactions of recently synthesized [Ni('S 5 ')], [Ni('OS 4 ')] 2 , [Ni('N H S 4 ')] 2 , [Ni('S 4 -C 5 ')] 2  and [Ni('S 4 -C 3 ')] were investigated ('OS 4 ' 2-  = 2,2'-bis(2-mercaptophenylthio)diethylether(2-), 'N H S 4 ' 2-  = 2,2'-bis(2-mercaptophenylthio)diethylamine(2-), 'S 5 ' 2-  = 2,2'-bis(2-mercaptophenylthio)diethylsulfide(2-), 'S 4 -C 5 ' 2-  = 1,5-bis(2-mercaptophenylthio)pentane(2-), 'S 4 -C 3 ' 2-  = 1,3-bis(2-mercaptophenylthio)propane(2-)).

zeitschrift für naturforschung b

Übergangsmetallkomplexe mit Schwefelliganden, LXXVIII. H + -, Lewis-Säure-Basen- und Ligandentransferreaktionen von Thioether-Thiolat-Nickelkomplexen. Röntgenstrukturanalysen von [Mo(O)(′OS 4 ′ )] und [Mo(O)(′N h S 4 ′)]/Transition Metal Complexes with Sulfur Ligands, LXXVIII. H + -, Lewis Acid-Base and Ligand Transfer Reactions of Thioether-Thiolato-Nickel Complexes. X-Ray Structure Determinations of [Mo(O)('OS 4 ')] and [Mo(O)('N H S 4 ')]