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Me 2 NC(S)SN(SiMe 3 ) 2  (1) reacts with TeCl 4  and NbCl 5  to yield Me 2 NC(S)SNTeCl 2  (4) and Me 2 NC(S)SNNbCl 3  (5), while the dithiocarbamate complexes 6 and 7 are formed with ZrCl 4  and HfCl 4 . The crystal structure of 6 is reported. The reaction of Me 2 NC(S)SN=TiCl 2 ·3 py 2 with LiN(SiMe 3 ) 2  gives the tricyclic compound 8.

zeitschrift für naturforschung b

Notizen: Reaktionen von Me 2 NC(S)SN(SiMe 3 ) 2  mit Metallhalogeniden — Kristallstruktur von Me 2 NCS 2 ZrCl 3  · 3 Pyridin / Reactions of Me 2 NC(S)SN(SiMe 3 ) 2  with Metal Halides – Crystal Structure of Me 2 NCS 2 ZrCl 3  · 3 Pyridine