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The title compound has been characterized by X-ray powder and single crystal diffraction: Pbcn; a = 7.296(1), b = 15.997(4), c = 7.016(1) Å; Z = 4; 1514 diffractometer data, R = 0.04, R w  = 0.03. The vibrational spectra are compatible with a tetrahedral geometry of the anion.

zeitschrift für naturforschung b

Synthese und Strukturanalyse des gemischten Alkalimetallorthonitrats Na 3 K 3 (NO 4 ) 2  / Synthesis and X-Ray Structure Determination of the Mixed Alkali Metal Orthonitrate Na 3 K 3 (NO 4 ) 2