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[Li(tmed)] 3 [Sm(CH 3 )6] reacts with tert-butanol in diethyl ether to give [Li 5 Sm(O–t-C 4 H 9 ) 8 ] (1), the structure of which has been elucidated by X-ray structure analysis. 1 crystallizes tetragonally with a = 1703(4) and c = 3178(1) pm, space group P4 1 2 1 2, Z = 8. The structure was refined to R = 0.042 for 4082 observed reflections (F o  &amp;gt; 6σ(F o )).

zeitschrift für naturforschung b

Metallorganische Verbindungen der Lanthanoide, 63 [1]. Pentalithium-okta-tert-butoxy-samarat(III): Synthese und Röntgenstrukturanalyse eines aus zwei flächenverknüpften Würfeln aufgebauten Lanthanoidclusters / Organometallic Compounds of the Lanthanoides, 63 [1]. Pentalithium Octa(tert-butoxy)samarat(III): Synthesis and X-Ray Structural Analysis of a Lanthanoid Cluster Made by Two Face Linked Cubes