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A heterogenized rhodium complex, prepared by sol-gel processing of Rh(CO)Cl[PPh 2 CH 2 CH 2 Si(OEt) 3 ] 2  and Si(OEt) 4 , is shown to catalyze the conversion of the silanes H 4-n SiPh„ (n = 1 - 3) or (HMe 2 Si) 2 O to (poly)siloxanes by air or water. Using THF as a solvent, the silanoles Ph 3 SiOH or Ph 2 Si(OH) 2  are obtained instead. The reaction of phenylacetic acid or acetic acid with HSiPh 3  to give silyl esters is catalyzed by the same compound.

zeitschrift für naturforschung b

Metallkomplexe in Anorganischen Matrices, 5 [1] / Metal Complexes in Inorganic Matrices, 5 [1]: Katalytische Silanoxidation an einem heterogenisierten Rhodium-Komplex /Catalytic Silane Oxidation at a Heterogenized Rhodium Complex