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[(PhCH 2 ) 2 InN(H)t-Bu] 2  (3) and [PhCH 2 (Cl)InN(SiMe 3 )2] 2  (4) have been prepared by the reaction of (PhCH 2 ) 2 InCl with LiN(H)t-Bu and of PhCH 2 InCl 2  with NaN(SiMe 3 ) 2 , respectively. 3 could be isolated in two isomers, while 4 forms only one chloro-bridged isomer in solution and in the solid state. The possibility of a chloro-bridged alkyl(aryl)chloroindium amide is also realized in [Mes(Cl)InN(SiMe 3 ) 2 ] 2  (2), as shown by X-ray analysis. The reaction of a 1:1-mixture of i-Pr 2 InCl/i-PrInCl 2  with LiN(H)t-Bu leads to all three possible compounds: [i-Pr(Cl)InN(H)t-Bu] 2  (1), {i-Pr 2 In[N(H)t-Bu] 2 In(Cl)i-Pr} (5), and [i-Pr 2 InN(H)t-Bu] 2  (6). Two isomers of the new compound 5 are detectable in solution. The crystal structure has been determined for the less sterically hindered isomer 5a, which forms hydrogen-bridged (Cl-H-N-bridge) infinite chains along the c-axis.

zeitschrift für naturforschung b

Synthese von Stickstoff- und Chlor-verbrückten Indiumorganylen. Die Kristallstrukturen von [Mes(Cl)InN(SiMe 3 ) 2 ] 2  und {i-Pr 2 In[N(H)t-Bu] 2 In(Cl)i-Pr} / Synthesis of Nitrogen- and Chloro-Bridged Organoindium Compounds. The Crystal Structures of [Mes(Cl)InN(SiMe 3 ) 2 ] 2  and {i-Pr 2 In[N(H)t-Bu] 2 In(Cl)i-Pr}