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By reacting PhAsCl 2  with NaC 5 H 5  in toluene under low temperature conditions PhAs(h 1 -C 5 H 5 ) 2  was obtained. Metallation of PhAs(h 1 -C 5 H 5 ) 2  with n-BuLi followed by reaction with TiCl 4  led to the As-bridged [1]titanocenophane. The structure and conformation of this air-stable compound are discussed in the light of its  1 H NMR spectrum.

PhAs(C 5 H 4 ) 2 TiCl 2 : Das erste Arsen-überbrückte Titanocenophan / PhAs(C 5 H 4 ) 2 TiCl 2 : The First Arsenic-Bridged Titanocenophane