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Ni(CNSiMe 3 ) 4  (Me = CH 3 ), the first homoleptic isocyanosilane complex, has been prepared by reaction of bis(1,5-cyclooctadiene)nickel(0) with trimethylcyanosilane in ether and characterized by its infrared, Raman spectra,  13 C NMR spectra.

zeitschrift für naturforschung b

Synthese und Eigenschaften von Tetrakis(trimethylsilylisocyanid)nickel(0), Ni(C=N—SiMe 3 ) 4  / Synthesis and Properties of Tetrakis(trimethylsilylisocyanide)nickel(0), Ni(C=N—SiMe 3 ) 4