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Cp*NbCl 4  (1) (Cp* = η 5 -C 5 Me 5 ) and (η 5 -C 5 EtMe 4 )NbCl 4  (2) are synthesized in moderate yields by reaction of NbCl 5  with the corresponding silanes.

zeitschrift für naturforschung b

Niob-Stickstoff-Verbindungen: Synthese und Struktur der Halbsandwichkomplexe Ph 3 P = N–Nb(η 5 -C 5 EtMe 4 )Cl 3  und [(η 5 -C 5 EtMe 4 )Cl 3 Nb–N = PPh 2 ] 2 C 2 H 2  / Niobium Nitrogen Complexes: Synthesis and Structure of Halfsandwich Complexes Ph 3 P=N–Nb(η 5 -C 5 EtMe 4 )Cl 3  and [(η 5 -C 5 EtMe 4 )Cl 3 Nb–N = PPh 2 ] 2 C 2 H 2