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Tricyansulfonium hexafluoroarsenate S(CN) 3  + AsF 6  -  is prepared by halide-pseudohalide exchange with SBr 3  + AsF 6  -  and AgCN. The cyandimethylsulfonium salts (CH 3 ) 2 SCN + AsF 6  -  and SbF 6  -  are obtained via reactions of CH 3 SCN with CH 3 OSO+MF 6  -  (M = As, Sb) in liquid SO 2 . The compounds are characterized by Raman, IR and NMR spectroscopy.

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Darstellung und spektroskopische Charakterisierung von Cyansulfoniumsalzen. S(CN) 3  + AsF 6 - und (CH 3 ) 2 SCN + MF 6 - (M = As, Sb) [1] / Preparation and Spectroscopic Characterization of Cyansulfonium Salts. S(CN) 3 +AsF 6 - and (CH 3 ) 2 SCN + MF 6 - (M = As, Sb) [1]