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1,1,3,3-Tetrakis(dimethylamino)-diphosphete (3) reacts with diphenylacetylene and bis(trimethylsilyl)butadiin-1 ,3 to give 1,1,3,3-tetrakis(dimethylamino)-4,5-diphenyl-1 λ 5 ,3λ 5 - diphosphorine (8) and 1,1,3,3-tetrakis(dimethylamino)-5-trimethylsilyl-4-(trimethylsilyl-ethinyl)-1λ 5 ,3 λ 5 -diphosphorine (9). The new compounds are characterized by their NMR , mass and IR spectra. In addition, the results of an X-ray structure analysis of 9 are reported.

1λ 5 ,3 λ 5 -Diphosphorine (1 λ 5 ,3 λ 5 -Diphosphabenzole), III [1, 2] / 1 λ 5 ,3 λ 5 -Diphosphorines (1 λ 5 ,3 λ 5 -Diphosphabenzenes), III [1, 2]