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The reaction of lithiated catechol ligands with W (0)Cl 4  produces LiCl as a side product. The lithium chloride from this reaction crystallizes as (THF) 2 Li(μ-Cl)-,Li(THF) 2 . The X -ray analysis shows lithium in the center of a distorted tetrahedron made up from two THF molecules and two bridging chlorides with d(Li-Cl) = 2.342(3) and 2.308(3)Å.

Synthese und Kristallstruktur von [LiCl · 2THF] 2 / Synthesis and Crystal Structure of [LiCl · 2THF] 2