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For the first time SF 5  containing organic phosphonates, SF 5 CF = CFP(O)(OR 1 ) 2  have been prepared from trimethylsilylphosphites, (R 1 O) 2 POSiMe 3  (R 1  = Et, R 1  = SiMe 3 ) and trifluorovinylsulfur pentafluoride, SF 5 CF = CF 2  in an Arbuzov type reaction.

I(E)-l,2-Difluoro-2-(pentafluoro-λ 6 -sulfanyl)ethenyl]phosphonates