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Reaction of 1-benzothiepine (4), whose synthesis has been improved, with trimethyloxonium tetrafluoroborate yields 1-methyl-1-benzothiepinium tetrafluoroborate (5). Compound 5 rearranges to methyl 1-naphthyl sulfide (6) on heating in acetonitrile. The reaction rate 5 → 6 was determined at one temperature (75°C).

zeitschrift für naturforschung b

Heterocyclische Siebenring-Verbindungen, XXXVII. Synthese und thermische Umlagerung von 1-Methyl- l -benzothiepinium-tetrafluoroborat / Heterocyclic Seven-Membered Ring Compounds, XXXVII. Synthesis and Thermal Rearrangement of 1 -Methyl-1-benzothiepinium Tetrafluoroborate